1AD4
DIHYDROPTEROATE SYNTHETASE COMPLEXED WITH OH-CH2-PTERIN-PYROPHOSPHATE FROM STAPHYLOCOCCUS AUREUS
Experimental procedure
Temperature [K] | 120 |
Collection date | 1996-08 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 65.748, 42.142, 99.040 |
Unit cell angles | 90.00, 106.06, 90.00 |
Refinement procedure
Resolution | 13.000 - 2.400 |
R-factor | 0.176 |
Rwork | 0.176 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.800 |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 13.000 * | |
High resolution limit [Å] | 2.400 * | 2.400 * |
Rmerge | 0.060 * | |
Total number of observations | 57389 * | |
Number of reflections | 19669 * | |
Completeness [%] | 93.0 * | 88 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 4 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG4000 | 12-16 (%(v/w)) | |
2 | 1 | reservoir | sodium potassium tartrate | 200 (mM) | |
3 | 1 | reservoir | bis-tris | 100 (mM) |