1ABY
CYANOMET RHB1.1 (RECOMBINANT HEMOGLOBIN)
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RUH2R |
Temperature [K] | 295 |
Detector technology | AREA DETECTOR |
Collection date | 1995-05 |
Detector | SIEMENS |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 102.540, 115.170, 56.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.600 |
R-factor | 0.175 |
Rwork | 0.175 |
R-free | 0.27800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | BML-3260 |
RMSD bond length | 0.009 |
RMSD bond angle | 20.620 * |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | AMoRE |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 115.000 | 2.800 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.056 | |
Total number of observations | 55634 * | |
Number of reflections | 19521 | |
Completeness [%] | 68.8 | 29.2 |
Redundancy | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 5 | pH 5.0 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 15 (mg/ml) | |
2 | 1 | drop | PEG3350 | 6.5 (%) | |
3 | 1 | drop | ammonium acetate | 75 (mM) | |
4 | 1 | drop | KCN | 0.25 (mM) | |
5 | 1 | reservoir | PEG3350 | 13 (%) | |
6 | 1 | reservoir | ammonium acetate | 150 (mM) | |
7 | 1 | reservoir | KCN | 10 (mM) |