Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 55.460, 71.820, 77.840 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.700 |
R-factor | 0.137 |
RMSD bond length | 0.016 |
RMSD bond angle | 0.044 |
Refinement software | PROLSQ |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Microdialysis * | 6.5 * | referred to 'Quiocho, F.A.', (1974) J.Mol.Biol., 86, 491-493 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | protein | ||
2 | 1 | 2 | MPD | 55 (%) | |
3 | 1 | 2 | potassium phosphate | 2 (mM) |