1A7B
ENGINEERING A MISFOLDED FORM OF CD2
Experimental procedure
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX7.2 |
Synchrotron site | SRS |
Beamline | PX7.2 |
Temperature [K] | 287 |
Detector technology | IMAGE PLATE |
Collection date | 1997-08 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 64.270, 80.030, 80.470 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.000 - 3.100 |
R-factor | 0.2389 |
Rwork | 0.239 |
R-free | 0.30600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1hng |
RMSD bond length | 0.005 |
RMSD bond angle | 1.272 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR (3.851) |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 | 2.150 |
High resolution limit [Å] | 2.000 | 2.080 |
Rmerge | 0.059 | 0.295 |
Number of reflections | 10589 | |
<I/σ(I)> | 16.1 | 2.57 |
Completeness [%] | 99.1 | 99 |
Redundancy | 2.89 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 7.5 | 2M AMMONIUM SULFATE 2% PEG 400, 0.1M HEPES, PH 7.5 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ammonium sulfate | 2 (M) | |
2 | 1 | reservoir | PEG400 | 2 (%) | |
3 | 1 | reservoir | glycerol | 10 (%) | |
4 | 1 | reservoir | NaHEPES | 0.1 (M) |