1A6V
B1-8 FV fragment complexed with a (4-hydroxy-3-nitrophenyl) acetate compound
Experimental procedure
| Source type | SYNCHROTRON |
| Source details | SRS BEAMLINE PX9.6 |
| Synchrotron site | SRS |
| Beamline | PX9.6 |
| Temperature [K] | 269 |
| Detector technology | IMAGE PLATE |
| Collection date | 1995-08 |
| Detector | MARRESEARCH |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 71.760, 86.190, 111.511 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 6.000 - 1.800 |
| Rwork | 0.296 |
| Structure solution method | MIR |
| RMSD bond length | 0.012 |
| RMSD bond angle | 0.040 |
| Data reduction software | MOSFLM |
| Data scaling software | Agrovata |
| Phasing software | MLPHARE |
| Refinement software | PROLSQ |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 9.200 | 1.880 |
| High resolution limit [Å] | 1.740 | 1.800 |
| Rmerge | 0.059 | 0.361 |
| Number of reflections | 367775 | |
| Completeness [%] | 94.8 | 95.8 |
| Redundancy | 5.9 | 3.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | CRYSTALS WERE GROWN USING AMMONIUM SULPHATE AS PRECIPITANT |
