1A3N
DEOXY HUMAN HEMOGLOBIN
Experimental procedure
Temperature [K] | 120 |
Detector technology | IMAGE PLATE |
Collection date | 1997-05 |
Detector | RIGAKU RAXIS II |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 62.650, 82.430, 53.530 |
Unit cell angles | 90.00, 99.61, 90.00 |
Refinement procedure
Resolution | 15.000 - 1.800 |
R-factor | 0.171 * |
Rwork | 0.171 |
R-free | 0.22038 |
RMSD bond length | 0.012 |
RMSD bond angle | 0.028 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.053 | 0.162 |
Number of reflections | 49661 | |
<I/σ(I)> | 15 | 4 |
Completeness [%] | 95.8 | 76.1 |
Redundancy | 2.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 6.5 * | Perutz, M.F., (1968) J. Cryst. Growth, 2, 54. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | ammonium sulfate | 4 (M) | |
2 | 1 | 1 | 2 (M) | ||
3 | 1 | 1 | 2 (M) |