1ZIL

GCN4-LEUCINE ZIPPER CORE MUTANT ASN16GLN IN THE DIMERIC STATE

Experimental procedure

Source type	SEALED TUBE
Detector technology	IMAGE PLATE
Collection date	1994-09
Detector	RIGAKU
Spacegroup name	C 1 2 1
Unit cell lengths	104.250, 30.790, 22.020
Unit cell angles	90.00, 95.57, 90.00

Refinement procedure

Resolution	6.000 - 2.250
R-factor	0.174 *
Rwork	0.174
RMSD bond length	0.010
RMSD bond angle	1.700
Data reduction software	R-AXIS
Data scaling software	R-AXIS
Refinement software	TNT

Data quality characteristics

	Overall
Low resolution limit [Å]	6.000 *
High resolution limit [Å]	2.250 *
Rmerge	0.086
Total number of observations	4794 *
Number of reflections	2627
Completeness [%]	65.0
Redundancy	1.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *		4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	peptide	20 (mg/ml)
2	1	reservoir		50 (mM)
3	1	reservoir		0.4 (M)
4	1	reservoir	PEG1450	2.5 (%)