1Z13
Crystal Structure of Bovine Low Molecular Weight PTPase Complexed with Molybdate
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 298 |
| Detector technology | IMAGE PLATE |
| Collection date | 1995-01-01 |
| Detector | RIGAKU RAXIS II |
| Wavelength(s) | 1.54 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 95.300, 43.400, 41.200 |
| Unit cell angles | 90.00, 113.40, 90.00 |
Refinement procedure
| Resolution | 20.000 - 2.200 |
| R-factor | 0.159 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1dg9 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 2.450 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | TNT |
| Refinement software | TNT |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.200 |
| Number of reflections | 5798 |
| Completeness [%] | 73.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 295 | PEG 4000, HEPES, Isopropanol, Na2MoO4, pH 7.5, VAPOR DIFFUSION, SITTING DROP, temperature 295K |
