1YW7

h-MetAP2 complexed with A444148

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU200
Temperature [K]	110
Wavelength(s)	1.54
Spacegroup name	C 2 2 21
Unit cell lengths	89.487, 98.735, 101.211
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	15.340 - 1.850
Rwork	0.218
R-free	0.24800
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	1.300
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	CNS
Refinement software	CNX (2002)

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	1.850
Number of reflections	38157
<I/σ(I)>	31.3
Completeness [%]	99.0
Redundancy	5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1