1YP3
Crystal structure of potato tuber ADP-glucose pyrophosphorylase in complex with ATP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 32-ID |
| Synchrotron site | APS |
| Beamline | 32-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-11-01 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.99997 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 79.581, 142.955, 90.438 |
| Unit cell angles | 90.00, 113.13, 90.00 |
Refinement procedure
| Resolution | 19.970 - 2.600 |
| R-factor | 0.175 |
| Rwork | 0.175 |
| R-free | 0.25500 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.300 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | CNS |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.760 |
| High resolution limit [Å] | 2.600 | 2.600 |
| Number of reflections | 43463 | |
| Completeness [%] | 76.3 | 97.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
