1YOC
Crystal Structure of genomics APC5556
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-BM |
| Synchrotron site | APS |
| Beamline | 19-BM |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-10-06 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.97943 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 88.162, 113.399, 58.838 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 40.830 - 1.700 |
| R-factor | 0.167 |
| Rwork | 0.167 |
| R-free | 0.20000 |
| Structure solution method | Sulfur SAD |
| RMSD bond length | 0.018 |
| RMSD bond angle | 2.100 |
| Data reduction software | DENZO |
| Data scaling software | HKL-2000 |
| Phasing software | SOLVE |
| Refinement software | CNS (1.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.760 |
| High resolution limit [Å] | 1.700 | 1.700 |
| Rmerge | 0.083 | 0.685 |
| Number of reflections | 59643 | |
| <I/σ(I)> | 7.5 | 2.47 |
| Completeness [%] | 99.3 | 93.6 |
| Redundancy | 9 | 8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | Na Formate, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
