1YM8
crystal structure of GZZ shows up puckering of the proline ring in the Xaa position.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.2.1 |
| Synchrotron site | ALS |
| Beamline | 8.2.1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-07-22 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.9800 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 23.230, 28.580, 80.510 |
| Unit cell angles | 90.00, 97.85, 90.00 |
Refinement procedure
| Resolution | 39.880 - 1.550 |
| R-factor | 0.2351 |
| Rwork | 0.235 |
| R-free | 0.25600 |
| Structure solution method | MIR |
| Starting model (for MR) | 1k6f |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.700 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | EPMR |
| Refinement software | CNS (1.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 39.880 | 1.650 |
| High resolution limit [Å] | 1.550 | 1.550 |
| Number of reflections | 15444 | |
| Completeness [%] | 100.0 | 99.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 277 | peg 400, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
