1YH3
Crystal structure of human CD38 extracellular domain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE F1 |
| Synchrotron site | CHESS |
| Beamline | F1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-07-20 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.916 |
| Spacegroup name | P 1 |
| Unit cell lengths | 41.839, 51.491, 66.439 |
| Unit cell angles | 108.27, 90.47, 97.29 |
Refinement procedure
| Resolution | 10.000 - 1.910 |
| R-factor | 0.19174 |
| Rwork | 0.188 |
| R-free | 0.25336 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.029 |
| RMSD bond angle | 2.264 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 1.930 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Number of reflections | 40203 | |
| Completeness [%] | 97.9 | 94.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 297 | MES, PEG4000, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 297K |
