1Y2F
Crystal Structure of ZipA with an inhibitor
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 44.973, 50.614, 84.399 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 43.410 - 2.000 |
| R-factor | 0.225 |
| Rwork | 0.225 |
| R-free | 0.22800 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1f46 |
| RMSD bond length | 0.021 |
| RMSD bond angle | 2.300 |
| Phasing software | AMoRE |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.090 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.108 | 0.399 |
| Number of reflections | 13540 | |
| <I/σ(I)> | 6.5 | 1.44 |
| Completeness [%] | 99.4 | |
| Redundancy | 4.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 6 | 298 | PEG 6000, MES, pH 6.0, VAPOR DIFFUSION, temperature 298.0K, pH 6.00 |
