1XWO

crystal structrue of goose delta crystallin

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2003-10-10
Detector	RIGAKU RAXIS IV
Wavelength(s)	1.542
Spacegroup name	P 1 21 1
Unit cell lengths	93.700, 99.000, 106.500
Unit cell angles	90.00, 101.40, 90.00

Refinement procedure

Resolution	20.000 - 2.800
R-factor	0.22
Rwork	0.210
R-free	0.28900
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.010
RMSD bond angle	1.300
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	MOLREP
Refinement software	CNS

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	2.850
High resolution limit [Å]	2.800	2.800
Rmerge	0.145
Number of reflections	45763
Completeness [%]	99.7	99.1
Redundancy	16.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.5	298	PEG 2000, magnesium chloride, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K