1XPQ
Crystal structure of fms1, a polyamine oxidase from yeast
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE A1 |
Synchrotron site | CHESS |
Beamline | A1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-08-06 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.94740 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 103.048, 98.133, 123.832 |
Unit cell angles | 90.00, 103.28, 90.00 |
Refinement procedure
Resolution | 42.930 - 2.510 |
R-factor | 0.202 |
Rwork | 0.200 |
R-free | 0.27610 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.500 |
Number of reflections | 66331 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 296 | 10% PEG 4000, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 296K |