1XMM
Structure of human Dcps bound to m7GDP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL40B2 |
| Synchrotron site | SPring-8 |
| Beamline | BL40B2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-11-25 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.9997 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 100.928, 105.140, 138.647 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.000 - 2.500 |
| R-factor | 0.21615 |
| Rwork | 0.214 |
| R-free | 0.26695 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.337 |
| Data reduction software | MOSFLM |
| Data scaling software | CCP4 ((SCALA)) |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 32.600 | 2.590 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Number of reflections | 51097 | |
| Completeness [%] | 99.9 | 98.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.4 | 298 | PEG3350, KH2PO4, NaCl, pH 4.4, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
