1XA6

Crystal Structure of the Human Beta2-Chimaerin

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 19-ID
Synchrotron site	APS
Beamline	19-ID
Temperature [K]	95
Detector technology	CCD
Collection date	2003-08-06
Detector	ADSC QUANTUM 4
Wavelength(s)	1.28
Spacegroup name	P 61 2 2
Unit cell lengths	131.090, 131.090, 288.750
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	20.000 - 3.200
R-factor	0.26
Rwork	0.252
R-free	0.29800
Structure solution method	SAD
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	SOLVE
Refinement software	CNS (1.0)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	3.300
High resolution limit [Å]	3.200	3.200
Rmerge	0.058
Number of reflections	26206
Completeness [%]	99.5	98.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.8	282	sodium/potassium phosphate, sodium cloride, ethanol, pH 6.8, VAPOR DIFFUSION, HANGING DROP, temperature 282.0K
1	VAPOR DIFFUSION, HANGING DROP	6.8	282	sodium/potassium phosphate, sodium cloride, ethanol, pH 6.8, VAPOR DIFFUSION, HANGING DROP, temperature 282.0K