1X24
Prl-1 (ptp4a)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X9A |
| Synchrotron site | NSLS |
| Beamline | X9A |
| Temperature [K] | 293 |
| Collection date | 2005-02-01 |
| Spacegroup name | I 21 3 |
| Unit cell lengths | 146.891, 146.891, 146.891 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 30.000 - 3.200 |
| Rwork | 0.241 |
| R-free | 0.28500 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | CNS |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 3.300 |
| High resolution limit [Å] | 3.200 | 3.200 |
| Number of reflections | 8744 | |
| Completeness [%] | 98.7 | 97.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 4.8 | 277 | 100mM AcNa, 2.0M Ammonium sulfate, pH 4.8, VAPOR DIFFUSION, temperature 277K |
