1WRI
Crystal Structure of Ferredoxin isoform II from E. arvense
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL44XU |
| Synchrotron site | SPring-8 |
| Beamline | BL44XU |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2002-12-18 |
| Detector | MACSCIENCE |
| Wavelength(s) | 0.9 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 97.544, 29.411, 32.561 |
| Unit cell angles | 90.00, 103.94, 90.00 |
Refinement procedure
| Resolution | 10.000 - 1.200 |
| R-factor | 0.1184 |
| Rwork | 0.109 |
| R-free | 0.14070 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.015 |
| RMSD bond angle | 0.033 |
| Data reduction software | MOSFLM |
| Data scaling software | CCP4 ((SCALA)) |
| Phasing software | CNS |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 16.500 | 1.240 |
| High resolution limit [Å] | 1.200 | 1.200 |
| Rmerge | 0.077 | |
| Number of reflections | 27366 | |
| <I/σ(I)> | 5.3 | |
| Completeness [%] | 97.2 | 97.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7.5 | 298 | Potassium phosphate, pH 7.5, VAPOR DIFFUSION, temperature 298K |
