1WMP
Crystal structure of amine oxidase complexed with cobalt ion
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL44XU |
| Synchrotron site | SPring-8 |
| Beamline | BL44XU |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2002-11-08 |
| Detector | Bruker DIP-6040 |
| Wavelength(s) | 0.9 |
| Spacegroup name | I 1 2 1 |
| Unit cell lengths | 157.580, 63.376, 184.204 |
| Unit cell angles | 90.00, 112.47, 90.00 |
Refinement procedure
| Resolution | 10.000 - 2.000 |
| R-factor | 0.19 |
| Rwork | 0.188 |
| R-free | 0.22000 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.300 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR (3.851) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 24.087 | 2.110 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.094 | |
| Number of reflections | 112241 | |
| Completeness [%] | 98.8 | 98.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | MICRODIALYSIS | 6.8 | 289 | 1.05M POTASSIUM SODIUM TARTRATE, 25mM HEPES, pH 6.8, MICRODIALYSIS, temperature 289K |
