1WM9
Structure of GTP cyclohydrolase I from Thermus thermophilus HB8
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL45PX |
| Synchrotron site | SPring-8 |
| Beamline | BL45PX |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2002-11-02 |
| Detector | RIGAKU |
| Wavelength(s) | 0.979 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 160.220, 110.477, 70.650 |
| Unit cell angles | 90.00, 105.27, 90.00 |
Refinement procedure
| Resolution | 50.000 - 2.200 |
| R-factor | 0.213 |
| Rwork | 0.208 |
| R-free | 0.26100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | CNS |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.200 |
| Number of reflections | 58232 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
