Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 113 |
| Detector technology | IMAGE PLATE |
| Collection date | 1997-07-03 |
| Detector | RIGAKU RAXIS IIC |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 64 2 2 |
| Unit cell lengths | 177.420, 177.420, 96.420 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 38.350 - 1.900 |
| R-factor | 0.15243 |
| Rwork | 0.152 |
| R-free | 0.17047 |
| Structure solution method | FOURIER SYNTHESIS |
| Starting model (for MR) | Published hexagonal structure without Mn or solvent atoms |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.280 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 1.970 | |
| High resolution limit [Å] | 1.900 | 1.900 |
| Number of reflections | 65584 | |
| <I/σ(I)> | 24.4 | 5.69 |
| Completeness [%] | 93.0 | 63.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8.3 | 277 | Tris, PEG 4k, pH 8.3, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
