1WK4
Crystal structure of ttk003001606
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL26B1 |
| Synchrotron site | SPring-8 |
| Beamline | BL26B1 |
| Detector technology | CCD |
| Collection date | 2004-04-11 |
| Wavelength(s) | 0.96500, 0.97897, 0.97933 |
| Spacegroup name | P 64 |
| Unit cell lengths | 78.332, 78.332, 197.038 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 47.190 - 2.800 |
| R-factor | 0.217 |
| Rwork | 0.217 |
| R-free | 0.27500 |
| Structure solution method | MAD |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.200 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SOLVE |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.900 |
| High resolution limit [Å] | 2.800 | 2.800 |
| Number of reflections | 33433 | |
| <I/σ(I)> | 30.7 | 2.1 |
| Completeness [%] | 99.9 | 100 |
| Redundancy | 16.8 | 17.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | MES, sodium formate, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 293.0K |
