1WE0
Crystal structure of peroxiredoxin (AhpC) from Amphibacillus xylanus
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-6A |
| Synchrotron site | Photon Factory |
| Beamline | BL-6A |
| Temperature [K] | 290 |
| Detector technology | IMAGE PLATE |
| Detector | FUJI |
| Wavelength(s) | 1.00 |
| Spacegroup name | P 1 |
| Unit cell lengths | 79.216, 79.319, 104.449 |
| Unit cell angles | 77.22, 82.33, 80.08 |
Refinement procedure
| Resolution | 50.000 - 2.900 |
| Rwork | 0.208 |
| R-free | 0.23500 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | CNS |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 3.000 |
| High resolution limit [Å] | 2.900 | 2.900 |
| Number of reflections | 46092 | |
| Completeness [%] | 83.6 | 55.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | PEG 6000, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | PEG 6000, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
