1WCE
Crystal structure of the T13 IBDV viral particle reveals a missing link in icosahedral viruses evolution
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-02-04 |
| Detector | MARRESEARCH |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 854.010, 692.230, 792.410 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 50.000 - 7.000 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1wcd |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | URO |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 7.700 |
| High resolution limit [Å] | 7.000 | 7.000 |
| Rmerge | 0.140 | 0.470 |
| Number of reflections | 1089650 | |
| <I/σ(I)> | 5.68 | 1.72 |
| Completeness [%] | 75.1 | 63.4 |
| Redundancy | 2.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.5 | 1.6% PEG8000 0.5M KSCN 100 MM HEPES PH7.5 20% GLYCEROL 20% MPD |
