1WAV
CRYSTAL STRUCTURE OF FORM B MONOCLINIC CRYSTAL OF INSULIN
Experimental procedure
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-6A |
| Synchrotron site | Photon Factory |
| Beamline | BL-6A |
| Detector technology | IMAGE PLATE |
| Collection date | 1994-05 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 49.240, 60.940, 48.180 |
| Unit cell angles | 90.00, 95.80, 90.00 |
Refinement procedure
| Resolution | 10.000 - 2.500 |
| R-factor | 0.206 |
| Rwork | 0.206 |
| RMSD bond length | 0.020 |
| RMSD bond angle | 3.858 |
| Data reduction software | WEIS |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 10.000 |
| High resolution limit [Å] | 2.500 |
| Rmerge | 0.063 |
| Number of reflections | 11200 |
| Completeness [%] | 91.0 |
| Redundancy | 4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
