1W8G
CRYSTAL STRUCTURE OF E. COLI K-12 YGGS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-10-08 |
Detector | ADSC CCD |
Spacegroup name | I 41 2 2 |
Unit cell lengths | 124.017, 124.017, 83.729 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.000 - 2.000 |
R-factor | 0.163 |
Rwork | 0.161 |
R-free | 0.19500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1b54 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.119 |
Data reduction software | DENZO |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.000 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.050 | 0.340 |
Number of reflections | 22295 | |
<I/σ(I)> | 34.2 | 5.9 |
Completeness [%] | 99.9 | 100 |
Redundancy | 9 | 9.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | 20% PEG 4000, 16% ISOPROPANOL, 0.1 M NA-CITRATE BUFFER PH 6, 5% SODIUM DEXTRANE SULPHATE |