1VTO
1.9 A RESOLUTION REFINED STRUCTURE OF TBP RECOGNIZING THE MINOR GROOVE OF TATAAAAG
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X25 |
Synchrotron site | NSLS |
Beamline | X25 |
Detector technology | IMAGE PLATE |
Detector | FUJI |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 42.000, 147.000, 57.000 |
Unit cell angles | 90.00, 90.50, 90.00 |
Refinement procedure
Resolution | 6.000 - 1.900 |
R-factor | 0.194 |
Rwork | 0.194 |
R-free | 0.26400 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.570 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 1.880 |
Number of reflections | 51793 |
Completeness [%] | 93.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.2 | 277 | pH 6.20, VAPOR DIFFUSION, temperature 277.00K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | 2 | 3 |
10 | 1 | 2 | MES | 29 | 30 |
2 | 1 | 1 | DTT | 5 | 6 |
3 | 1 | 1 | GLYCEROL | 8 | 9 |
4 | 1 | 1 | MES | 11 | 12 |
5 | 1 | 1 | KCL | 14 | 15 |
6 | 1 | 1 | NH4 ACETATE | 17 | 18 |
7 | 1 | 2 | WATER | 20 | 21 |
8 | 1 | 2 | DTT | 23 | 24 |
9 | 1 | 2 | GLYCEROL | 26 | 27 |