1VRH
HRV14/SDZ 880-061 COMPLEX
Experimental procedure
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE A1 |
| Synchrotron site | CHESS |
| Beamline | A1 |
| Detector technology | FILM |
| Collection date | 1990-06 |
| Spacegroup name | P 21 3 |
| Unit cell lengths | 445.100, 445.100, 445.100 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | ? - 3.000 |
| Data reduction software | PURDUE (DATA PROCESSING PACKAGE) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 * | |
| High resolution limit [Å] | 3.000 * | 3.000 * |
| Rmerge | 0.119 | 0.195 * |
| Number of reflections | 147189 * | 35847 * |
| Completeness [%] | 25.8 * | 16 * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 7.2 * | 5 MG/ML OF SDZ 880-061 IN 200 MICROLITER DROPS FOR 3 - 4 CRYSTALS |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | virus | 5 (mg/ml) | |
| 2 | 1 | drop | Tris-HCl | 5 (mM) | |
| 3 | 1 | drop | PEG8000 | 0.125-0.375 (%(w/v)) | |
| 4 | 1 | drop | 10 (mM) | ||
| 5 | 1 | reservoir | Tris-HCl | 10 (mM) | |
| 6 | 1 | reservoir | PEG8000 | 0.25-0.75 (%(w/v)) | |
| 7 | 1 | reservoir | 20 (mM) |
