1VKL
RABBIT MUSCLE PHOSPHOGLUCOMUTASE
Experimental procedure
| Temperature [K] | 289 |
| Detector technology | AREA DETECTOR |
| Collection date | 1993-10 |
| Detector | XUONG-HAMLIN MULTIWIRE |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 174.420, 174.420, 101.120 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 6.000 - 2.700 |
| R-factor | 0.17 |
| Rwork | 0.170 |
| R-free | 0.21000 |
| Starting model (for MR) | 3pmg |
| RMSD bond length | 0.013 |
| RMSD bond angle | 24.543 * |
| Data reduction software | XDS |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 2.600 |
| Rmerge | 0.150 |
| Number of reflections | 46280 |
| Completeness [%] | 97.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 6.4 | Lin, Z., (1986) J.Biol.Chem., 261, 264. * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | ammonium salfate | 47 (%sat) | |
| 2 | 1 | 1 | PEG400 | 3-4 (%) |
