1V8L
Structure Analysis of the ADP-ribose pyrophosphatase complexed with ADP-ribose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.54 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 49.771, 49.771, 119.330 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 16.140 - 2.100 |
R-factor | 0.217 |
Rwork | 0.217 |
R-free | 0.24000 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 2.000 |
Phasing software | AMoRE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.120 |
High resolution limit [Å] | 2.010 | 2.010 |
Number of reflections | 11986 | |
Completeness [%] | 99.9 | 99.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |