1V6Z
Crystal structure of TT1573 from Thermus thermophilus
Experimental procedure
Experimental method | SAD |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44B2 |
Synchrotron site | SPring-8 |
Beamline | BL44B2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-10-02 |
Detector | MARRESEARCH |
Wavelength(s) | 0.9790 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 54.406, 78.506, 54.871 |
Unit cell angles | 90.00, 114.43, 90.00 |
Refinement procedure
Resolution | 49.960 - 2.000 |
Rwork | 0.197 |
R-free | 0.24600 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 1.400 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.960 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 28450 | |
<I/σ(I)> | 39 | 15.4 |
Completeness [%] | 99.9 | 99.4 |
Redundancy | 9.8 | 5.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 297 | 25% PEG3350, 0.2M Potassium Formate, VAPOR DIFFUSION, HANGING DROP, temperature 297K |