1V3Q
Structure of human PNP complexed with DDI
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | LNLS BEAMLINE D03B-MX1 |
Synchrotron site | LNLS |
Beamline | D03B-MX1 |
Temperature [K] | 104 |
Detector technology | CCD |
Collection date | 2003-04-16 |
Detector | MARRESEARCH |
Wavelength(s) | 1.431 |
Spacegroup name | H 3 2 |
Unit cell lengths | 141.330, 141.330, 161.450 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 2.800 |
R-factor | 0.214 |
Rwork | 0.214 |
R-free | 0.30600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1m73 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.830 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 56.796 | 2.950 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 46457 | |
<I/σ(I)> | 7.5 | 1.3 |
Completeness [%] | 91.0 | 96 |
Redundancy | 5.5 | 5.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.3 | pH 5.30 |