1V00
Erythrina cristagalli lectin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX14.1 |
Synchrotron site | SRS |
Beamline | PX14.1 |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2002-02-15 |
Detector | ADSC CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 54.900, 167.230, 55.130 |
Unit cell angles | 90.00, 97.08, 90.00 |
Refinement procedure
Resolution | 21.120 - 1.700 |
R-factor | 0.172 |
Rwork | 0.172 |
R-free | 0.19500 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.490 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.760 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.058 | 0.134 |
Number of reflections | 108695 | |
<I/σ(I)> | 28.09 | 5.28 |
Completeness [%] | 99.9 | 77.3 |
Redundancy | 1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 20% PEG 3350, 0.2M IMIDAZOLE, pH 7.00 |