1UOW
Calcium binding domain C2B
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 14-BM-C |
| Synchrotron site | APS |
| Beamline | 14-BM-C |
| Temperature [K] | 100 |
| Collection date | 2003-05-15 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 54.550, 54.550, 103.590 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 20.000 - 1.040 |
| R-factor | 0.16658 |
| Rwork | 0.166 |
| R-free | 0.18352 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1k5w |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 1.060 |
| High resolution limit [Å] | 1.040 | 1.040 |
| Rmerge | 0.103 | 0.416 |
| Number of reflections | 4126 | |
| <I/σ(I)> | 19.34 | 1.62 |
| Completeness [%] | 99.0 | 96.6 |
| Redundancy | 5.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5 | pH 5.00 |
