1UOV
Calcium binding domain C2B
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU R-AXIS |
Temperature [K] | 100 |
Collection date | 2003-05-15 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 54.678, 54.678, 103.767 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 1.650 |
R-factor | 0.16371 |
Rwork | 0.162 |
R-free | 0.19585 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1k5w |
Data scaling software | SCALEPACK |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.690 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.095 | 0.386 |
Number of reflections | 22306 | |
<I/σ(I)> | 24.18 | 4.13 |
Completeness [%] | 99.9 | 98.7 |
Redundancy | 7.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5 | pH 5.00 |