1UOV
Calcium binding domain C2B
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU R-AXIS |
| Temperature [K] | 100 |
| Collection date | 2003-05-15 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 54.678, 54.678, 103.767 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 20.000 - 1.650 |
| R-factor | 0.16371 |
| Rwork | 0.162 |
| R-free | 0.19585 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1k5w |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 1.690 |
| High resolution limit [Å] | 1.650 | 1.650 |
| Rmerge | 0.095 | 0.386 |
| Number of reflections | 22306 | |
| <I/σ(I)> | 24.18 | 4.13 |
| Completeness [%] | 99.9 | 98.7 |
| Redundancy | 7.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5 | pH 5.00 |
