1UNY
Structure Based Engineering of Internal Molecular Surfaces Of Four Helix Bundles
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 114 |
Collection date | 2002-10-15 |
Spacegroup name | P 41 3 2 |
Unit cell lengths | 79.348, 79.348, 79.348 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.900 - 2.300 |
R-factor | 0.2273 |
Rwork | 0.253 |
R-free | 0.32202 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | CrystalClear ((MSC/RIGAKU)) |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 26.300 |
High resolution limit [Å] | 2.000 |
Rmerge | 0.140 |
Number of reflections | 4127 |
<I/σ(I)> | 3.4 |
Completeness [%] | 100.0 |
Redundancy | 18.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 2.5 M NACL, 100 MM NAAC, 200 MM LI2SO4, PH 4.5 |