1ULS
Crystal structure of tt0140 from Thermus thermophilus HB8
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL45XU |
Synchrotron site | SPring-8 |
Beamline | BL45XU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2001-11-07 |
Detector | RIGAKU RAXIS V |
Wavelength(s) | 1.020 |
Spacegroup name | P 1 |
Unit cell lengths | 77.260, 77.330, 78.670 |
Unit cell angles | 90.12, 90.96, 95.12 |
Refinement procedure
Resolution | 46.400 - 2.400 |
R-factor | 0.196 |
Rwork | 0.196 |
R-free | 0.25200 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.300 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 69802 | |
Completeness [%] | 98.2 | 95.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | VAPOR DIFFUSION, HANGING DROP |