1U3P
IspF native
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2001-04-02 |
Detector | MARRESEARCH |
Wavelength(s) | 1.541 |
Spacegroup name | I 21 3 |
Unit cell lengths | 144.150, 144.150, 144.150 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.850 |
R-factor | 0.23 |
Rwork | 0.226 |
R-free | 0.23700 |
Structure solution method | MIR |
RMSD bond length | 0.012 |
RMSD bond angle | 1.840 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MLPHARE |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.850 |
Rmerge | 0.074 |
Number of reflections | 11403 |
Completeness [%] | 97.4 |
Redundancy | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | ammonium formate, pH 7, VAPOR DIFFUSION, SITTING DROP, temperature 293K |