1U0Q
Structure of a Llama VHH domain raised against a carbazole molecule
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2001-04-05 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.988 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 48.235, 48.235, 163.983 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.000 - 1.600 |
R-factor | 0.221 |
Rwork | 0.221 |
R-free | 0.25000 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.270 |
Data reduction software | DENZO |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.000 | 1.700 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.045 | 0.114 |
Number of reflections | 28590 | |
<I/σ(I)> | 8.3 | 6.3 |
Completeness [%] | 90.4 | 63 |
Redundancy | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.2 | 293 | PEG 5000 30%, AmSO4 200mM, pH 7.2, VAPOR DIFFUSION, HANGING DROP, temperature 293K |