1TZA
X-ray structure of Northeast Structural Genomics Consortium target SoR45
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X4A |
| Synchrotron site | NSLS |
| Beamline | X4A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-06-24 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.97868 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 51.947, 72.287, 75.574 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 29.670 - 2.400 |
| R-factor | 0.221 |
| Rwork | 0.217 |
| R-free | 0.26800 |
| Structure solution method | SAD |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.400 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.490 |
| High resolution limit [Å] | 2.400 | 2.400 |
| Rmerge | 0.050 | 0.073 |
| Number of reflections | 10666 | |
| <I/σ(I)> | 52.23 | 37.83 |
| Completeness [%] | 92.3 | 99.1 |
| Redundancy | 8.93 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5 | 8% PEG4000, 0.05mM Cacodylic Acid, pH 5.0, VAPOR DIFFUSION, HANGING DROP |
