1TRO
CRYSTAL STRUCTURE OF TRP REPRESSOR OPERATOR COMPLEX AT ATOMIC RESOLUTION
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 43.650, 72.430, 107.390 |
| Unit cell angles | 90.00, 94.96, 90.00 |
Refinement procedure
| Resolution | 10.000 - 2.400 * |
| R-factor | 0.249 * |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.300 |
| Refinement software | PROLSQ |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 10.000 * |
| High resolution limit [Å] | 2.400 * |
| Rmerge | 0.110 * |
| Completeness [%] | 87.3 * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | VAPOR DIFFUSION |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER | ||
| 2 | 1 | 1 | MPD | ||
| 3 | 1 | 1 | NACL | ||
| 4 | 1 | 1 | CACL2 | ||
| 5 | 1 | 1 | NA CACODYLATE |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | 2,4-dimethyl pentanediol | 35 (%) | |
| 2 | 1 | reservoir | 50 (mM) | ||
| 3 | 1 | reservoir | 11 (mM) | ||
| 4 | 1 | reservoir | cacodylate | 10 (mM) |
