1TQ2
Crystal Structure of IIGP1: a paradigm for interferon inducible p47 resistance GTPases
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-10-26 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.939 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 81.860, 92.670, 142.400 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.700 |
R-factor | 0.24 |
Rwork | 0.222 |
R-free | 0.28000 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.240 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | AMoRE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.770 |
High resolution limit [Å] | 2.700 | 2.700 |
Number of reflections | 28431 | |
<I/σ(I)> | 8.3 | 4.7 |
Completeness [%] | 92.6 | 92.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.5 | 293 | PEG 20000, MES, pH 6.5, VAPOR DIFFUSION, temperature 293K |