1TPH

1.8 ANGSTROMS CRYSTAL STRUCTURE OF WILD TYPE CHICKEN TRIOSEPHOSPHATE ISOMERASE-PHOSPHOGLYCOLOHYDROXAMATE COMPLEX

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	136.400, 74.000, 57.200
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 1.800
R-factor	0.185
RMSD bond length	0.017
RMSD bond angle	0.034
Refinement software	PROLSQ

Data quality characteristics

	Overall
Low resolution limit [Å]	13.000 *
High resolution limit [Å]	1.800 *
Number of reflections	50153 *
Completeness [%]	95.0 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	phosphoglycolohydroxamate phosphate		saturating amounts
2	1	drop	PEG		wide concentration
3	1	reservoir	Tris	100 (mM)
4	1	reservoir	PEG8000	12.5-21.0 (%(w/v))
5	1	reservoir	lithium	200 (mM)