1TNR

CRYSTAL STRUCTURE OF THE SOLUBLE HUMAN 55 KD TNF RECEPTOR-HUMAN TNF-BETA COMPLEX: IMPLICATIONS FOR TNF RECEPTOR ACTIVATION

Experimental procedure

Spacegroup name	I 2 3
Unit cell lengths	145.640, 145.640, 145.640
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.000 - 2.850
R-factor	0.16
Rwork	0.160
RMSD bond length	0.012
RMSD bond angle	1.800
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.830 *
Rmerge	0.078 *
Total number of observations	43171 *
Number of reflections	13270 *
Completeness [%]	99.7 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG4000	15 (%)
2	1	reservoir		200-400 (mM)
3	1	reservoir	beta-octyl glucoside	2 (%)
4	1	reservoir	sodium cacodylate	100 (mM)