1TLX
THERMOLYSIN (NATIVE)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 293 |
| Detector technology | IMAGE PLATE |
| Collection date | 1996-12-01 |
| Detector | MAR scanner 300 mm plate |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 93.910, 93.910, 131.170 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 20.000 - 2.100 |
| Rwork | 0.153 |
| R-free | 0.21400 |
| Structure solution method | ISOMORPHOUS REPLACEMENT |
| RMSD bond length | 0.014 |
| RMSD bond angle | 0.035 |
| Data reduction software | DENZO |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.240 |
| High resolution limit [Å] | 2.100 | 2.100 |
| Rmerge | 0.123 | 0.386 |
| Number of reflections | 20252 | |
| <I/σ(I)> | 4.9 | 2 |
| Completeness [%] | 99.0 | 98 |
| Redundancy | 14.9 | 15 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 7.5 | This particular structure is not described in this paper. * |
