1TCX
HIV TRIPLE MUTANT PROTEASE COMPLEXED WITH INHIBITOR SB203386
Experimental procedure
| Collection date | 1993 |
| Detector | SIEMENS |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 59.600, 87.500, 47.000 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 2.300 |
| R-factor | 0.18 |
| Rwork | 0.180 |
| RMSD bond length | 0.016 |
| RMSD bond angle | 27.200 * |
| Data reduction software | XENGEN |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 8.000 |
| High resolution limit [Å] | 2.300 |
| Rmerge | 0.074 |
| Number of reflections | 9902 |
| Completeness [%] | 85.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 5 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | ammonium sulfate | 20 (%sat) | |
| 2 | 1 | reservoir | sodium acetate | 0.2 (M) |
