1TCW
SIV PROTEASE COMPLEXED WITH INHIBITOR SB203386
Experimental procedure
| Collection date | 1993 |
| Detector | SIEMENS |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 56.100, 41.500, 53.100 |
| Unit cell angles | 90.00, 99.60, 90.00 |
Refinement procedure
| Resolution | 7.000 - 2.400 |
| R-factor | 0.197 |
| Rwork | 0.197 |
| RMSD bond length | 0.018 |
| RMSD bond angle | 29.710 * |
| Data reduction software | XENGEN |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.400 * |
| Rmerge | 0.074 |
| Number of reflections | 10269 |
| Completeness [%] | 93.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 4.2 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | 25-30 (%) | ||
| 2 | 1 | reservoir | sodium acetate | 100 (mM) |
