1TBQ

CRYSTAL STRUCTURE OF INSECT DERIVED DOUBLE DOMAIN KAZAL INHIBITOR RHODNIIN IN COMPLEX WITH THROMBIN

Experimental procedure

Detector technology	IMAGE PLATE
Collection date	1993-12-18
Detector	MARRESEARCH
Spacegroup name	P 21 21 21
Unit cell lengths	91.311, 111.600, 112.140
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 3.100
R-factor	0.175
Rwork	0.175
RMSD bond length	0.010
RMSD bond angle	1.620
Data reduction software	MOSFLM
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	999.000
High resolution limit [Å]	3.100	3.100 *
Rmerge	0.062 *
Total number of observations	31602 *
Number of reflections	16957
Completeness [%]	79.1 *	82.3 *
Redundancy	1.86

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	6 *	20 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG4000	10 (%)
2	1	reservoir	phosphate	300 (mM)